ICP20000

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Product Code: 6695
Brand: ICP
ICP-20000


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ICP20000 Inductively Coupled Plasma Atomic Emission Spectrometer is a powerful performance.   simultaneous

full- spectrum direct-reading spectrometer developed by Acculab USA , which is used for trace elemental analysis in diverse samples (soluble in hydrochloric acid, nitric acid , hydrofluoric acid, etc.. )   .

The instrument offers capabilities with automatization, stability, reliability and ease of use   .

It is currently widely applies in various fields of rare earth, geological, melallurgical, chemical, enviromental, clinicL MEDICINE, petroleum, semiconductor, food, biological samples, criminal science and   agricultural

research, etc..

Application Fields:

Characteristic :

  • Silicon industrial magnetic materials.
  • Metallurgical analyze As, Bi, Pb, Sb, Sn and other impurity elements which effect greatly the metalic materials quality.
  • Water analysis: analyze 8 heavy metal elements.
  • Geological, minera: analyze Ca, Mg, Na, Fe, Cu, Mn, Zn, Co, Ni, Nu, Ag and other elements in the rock samples.
  • Petrochemical and industrial: Analyze over 30 elements in crude oil, mainly Fe,Na, Mg, Ni, V, Ca, Pb, Mo, Mn, Cr, Co, Ba, As, etc..

•Pharmaceutical, health, agricultural, enviromental and Food safety.

Advantage

Full automation design :

The instrument is thoroughly computer-controlled except the power switch, which is reliable, safe and convenient .

Auto-control of gas flow :

in the sample introduction system, the carier gas, plasma gas, auxiliary gas are controlled through the advanced mass flow controller (MFC). Features continuosly adjustable and stable, etc. , which ensures the stability of the introduction system and the foundation for the stable light source.

Peristaltic pump :

A high precision 12 roller , 4 channel peristaltic pump , with speed adjustable according to the demanding, provides smooth, stable sample introduction and drain, to ensure the introduction rate consistent with the drain rate, which is adjusted as per required to stabilize the introduction system.

Precise wavelength positioning :

Intelligent precise automatic wavelength calibration algorithm, achieves the measurment without additional peaks calibration to ensure an accurate measurment time.

Stable, advanced solid-state RF power :

The instrument employs the solid-state RF power developed by Acculab Usa Instrument Co. , which is compact and delivers reliable performance with the power stability and safety, to further improve the instrument’s stability and security.

Superb optical system :

Adopting the echelle-prsm cross-dispersion type polychromator, elegant optical oplimization design maximizes the flux whilst enabling the exceltent spectral resolution. No movable optical components achieves unparalleled

long-term stability: Uitra-low stray light design with the unique optical design greatty reduces the background interference and further improves the detection llmit. A nighly efficient N.distributed purge system for the optical tank combined with the high-quality optics ensures deep UV analysis. especially P. S.As. etc..

Excellent pertormance detector :

Employing the CID detector which is advanced,mature and stable. largest size active area.megapixel. Full-frame Imaging ability to capture the entire ICP-OES spectrum (165-900 nm) permits quantitative analysis Non-destruetive readout improves the signal-to-noise rabo of weak analyte lines and ensures the precision of results. whst enabling cata acqurement and anaysis faster than CCD Excellent linear dynamic range and inherent anti-blooming capability aliow the measurement of wuak analyte emission signals adjacent to intense emission signals. whilst providing flexibility to choose the ideal wavelength for a method fallemative secondary and tertiary lines to overcome interferences)

Fast,accutate auto-matching :

The load terminals employs the fuil-automatic matching technology developed by Acculab Instrument Co.,Ltd., features fast matching.high precision. etc,which could achieve maximum output power. enhance power efficiency, ensure the stability of the instrument whilst facilitating ignition.

Ultra-fast analysis speed :

The analyst can set any suitable integration time for all the analytical lines in one exposure to achieve optimal measurement. or acquire the intensity integral value in the end of the exposure to enable the analysis faster, or specify any one or several specific Line(s)to read-out (the read-out time<2ms)

Powerful software analysis function :

Software is easy to operate and intuitive, it offers the capability with qualitative, semi-quantitative and quantitative analysis, instrument diagnostics. Intelligent optimization, flexible full-spectrum research function, strong offline reprocessing. Scientifically intelligence background correction and interference cancellation algorithm. Which enable the analysis more professional and accurate.

Advanced sample introduction system :

The sample introduction system is efficient and stable, equipped with various nebulizers and spray chambers, it can also be equipped with high solids nebulizer. Hydrogen fluoride-resistant nebulize0.etc.as per required. Besides the auto sampler developed by Acculab facilitates the operation. And further improves the analysis efficiency.

 

TECHNICAL SPECIFICATION

RF Generator Technical Specifications
Input Power

AC 220V,20A

Output power

700-1600W

Accuracy

2W

Working Frequency

27.12MHz

Frequency stability

   <0.05%

Output power stability

<0.1%

Match method

  auto-matching

Electromagnetic leakage radiation intensity 

electric field Intensity E <0.5V / m at 30cm away from the chamber

Introduction sample system technical specifications
Output coil

Inner-diameter 25mm,3 turns

 

Quartz tri-concentric torch

Outer-diameter 20mm.Various center channel size models optional

High-efficient nebulizer 

Concentric nebulizer outer-diameter 6mm. Vvarious models(high-salt,anti-

Spray chamber 

Scott spray chamber, the cyclonic spray chamber with outer diameter 57.2mm

Peristaltic pump 

12-roller, 4-channel, the rotation speed can be adjusted according to the demanded flow

Total consumption(Ar) 

<14L min

Plasma gas flow meter(100-1000)L/h(1.6 16L/min)

Argon flow meter/carrie

Auxiliary gas flow meter(6-60)L/h(0.1-1L/min)

gas pressure gauge 

Carrier gas flow meter(6-60)L/h(0.1-1L/min)

specifications

Carrier gas regulator valve (0.2MPa)

Cooling water: Water temp. 20-25’℃ Flow> 5L/min Pressure> 0.1MPa

spectrometer
 

Ruled echelle grating

52,67 lp/mm, 64°blaze angle, the substrate is made of high efficiency material

Ruled echelle grating

Prism

Ultra-pure Corning UV fused silica, transmittance %99.6 at 170nm

 

Wavelength range

175nm~900nm for standard, extended to 165nm900-nm by choosing DUV optical

 

Effective Focal length

430mm

Numerical aperture 

F/8,ultra-high flux ensures the instrument detection limit and sensitivity

 

Resolution

0.0068nm@200nm

Stray light

Equivalent background concentration of 10000ppmCa solution <2ppm at

Optical chamber

Precisely thermostat,0.1±35C Distributed N2 purge: normal purge 2Limin,fast purge 4L/min

Detection device Technical Specifications
Detector Type

Charge injection detector (CID)

 

Pixel Size

27×27μm,Random Access Integration (RAI)

Read mode

Full frame readout (FF), Random Access Integration (RAI) with non-destructive read

Linear dynamic range

(NDRO)10

Wavelength response range

165nm-1000nm

 

Electronic shutter

Set the integrationtime of each line; specify the individual line to read out(read time

Quantum efficiency

No coating. Up to 35% wtithin 200nm UV region

Detector cooling

 

 

High efficiency triple stage thermoelectric cooling device maintains the detector at a con-

Instrument Specifications
View mode

Radial view

Liquid content

0.01ppm-several thousands ppm

Solid content

0.001%-70%

Repeatability

(short-term stability) relative standard deviation RSD <0.5%

Stability

Relative standard deviation RSD <1% within 2 Hours

Analysis speedSingle line CID readout time is 2ms. analysis for all elements can be achieved within one
Detection limit(ug/L)

Detection limit(ug/L)

Instrument size          Desktop1300mm*840mm*740mm

 

Typical detection limit of elements
ElementAg

Ba

Be             Ca              Cr              Cu               K                 Li                Mg

Wavelength328.068455.403

311.107   393.366   267.716   324.754   766.49      670.784    279.553

Detection limit1.310.1

0.06          0.02          13              1.1              4.9             0.2              0.05

ElementMnMo

Na             Ni              Sr               Ti                V                 Zn

Wavelength

257.61

202.03

589.592   231.604   407.771   336.121   309.311    213.856

Detection limi

0.22

1.11

1.43          2.19          0.034        0.42           0.88           0.47

Instrument configuration

Working environment

Fully automated matcher

Manual

Store&transport temp.:15℃-25℃        Power adaptability

The sample introduction

system

Detection device

Store&transport relative                   220±10V.

humidity:<70%

Fully automated solid-state

RF power

Spectrometer

Working humidity:<70%                   50-60Hz

Auto-controlled cooling water apparatus

Computer system

Working temp.:15℃-30℃

 

 

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